New SUZ-4 Zeolite Membrane from Sol-Gel Technique

نویسندگان

  • P. Worathanakul
  • P. Kongkachuichay
چکیده

A new SUZ-4 zeolite membrane with tetraethlyammonium hydroxide as the template was fabricated on mullite tube via hydrothermal sol-gel synthesis in a rotating autoclave reactor. The suitable synthesis condition was SiO2:Al2O3 ratio of 21.2 for 4 days at 155 °C crystallization under autogenous pressure. The obtained SUZ-4 possessed a high BET surface area of 396.4 m/g, total pore volume at 2.611 cm/g, and narrow pore size distribution with 97 nm mean diameter and 760 nm long of needle crystal shape. The SUZ-4 layer obtained from seeding crystallization was thicker than that of without seeds or in situ crystallization. Keywords—Membrane, seeding, sol-gel, SUZ-4 Zeolite.

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تاریخ انتشار 2012